Journal of the Korean Ceramic Society (한국세라믹학회지)

The Korean Ceramic Society (한국세라믹학회)
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Preparation of Spherical $TiO_2$Powders by Spray Pyrolysis Using Ultrasonic Atomization Technique

초음파 분무 열분해법에 의한 구형 $TiO_2$ 미분말의 합성

  • 이종흔 (서울대학교 공과대학 무기재료공학과) ;
  • 조형진 (서울대학교 공과대학 무기재료공학과) ;
  • 박순자 (서울대학교 공과대학 무기재료공학과)
  • Published : 1991.10.01
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Abstract

Spherical TiO2 particles are prepared from TiCl4 aqueous solution by the spray pyrolysis method using ultrasonic atomization technique. The formation mechanism of TiO2 particles from atomized droplets it studied by varying the concentration of the source solution, reaction temperature, and the solvent. spherical TiO2 powders with almost the same normalized particle size distribution can be made reproducibly by changing the concentration of the source solution, and their mean sizes are in the range of 0.2~1.4${\mu}{\textrm}{m}$.

Keywords

References

  1. J. Am. Cer. Soc. v.72 no.4 Preparation of Fine, Spherical Yttria-stabilized Zirconia by the Spray Pyrolysis Method B. Dubois;R. Ruffier;P. Odier
  2. Advances in Ceramics: Ceramic Powder Sciene v.21 Ceramic Powder Synthesis by Thermal Reaction of Atomized Solutions D.W. Sproson;G.L. Messing
  3. Am. Cer. Soc. Bull. v.65 no.10 Homogeneous Y₂O₃-Stabilized ZrO₂ Powder by Spray Pyrolysis Method H. Ishizawa;O. Sakurai;N. Mizutani;M. Kato
  4. J. Am. Cer. Soc. v.73 no.1 Synthesis of Solid, Zirconia Paricles by Spray Pyrolysis S.C. Zhang;G.L. Messing
  5. Ceramic Powder Science Ⅲ Solid Particle Formation During Spray Pyrolysis S.C. Zhang;G.L. Messing;G.L. Messing(ed.);S. Hirano(ed.);H. Hausner(ed.)
  6. Ceramic Powder Science Ⅲ Processing of Ceramic Powders by Spray Pyrolysis Method; Influence of the Precursors. Examples of zirconia and YBa₂Cu₃$O_7$ P. Odier;B. Dubois;C. Clinard;H. Stroumbos;Monod;G.L. Messing(ed.);S. Hirano(ed.);H. Hausner(ed.)
  7. Ceramic Powder Science Ⅲ Synthesis of Spherical Si₃N₄ Powders by Spray Pyrolysis of Polysilazane N. Mizutani;T.Q. Liu;G.L. Messing(ed.);S. Hirano(ed.);H. Hausner(ed.)
  8. Am. Cer. Soc. Bull. v.56 no.11 Preparation of Fine Oxide Powders by Evaporative Decomposition of Solutions D.M. Roy;R.R. Neurgaonkar;T.P. O'Holleran;R. Roy
  9. Ceramics International v.12 Powder Synthesis of Electronic Ceramics by Evaporative Decomposition of Solutions D.W. Sproson;G.L. Messing;T.J. Gardner
  10. J. Colloid Interface Sci. v.68 no.2 Preparation of Uniform Colloidal Dispersions by Chemical Dispersions by Chemical Reactions in Aerosols: Ⅰ. Spherical Particles of Titanium Dioxide M. Visca;E. Matijevic
  11. J. Colloid Interface Sci. v.34 no.4 A New Liquid Aerosol Generator G. Nicolaon;D.D. Cooke;M. Kerker;E. Matijevic
  12. J. Acoustical Soc. Amer. v.34 no.1 Ultrasonic Atomization of Liquids R.J. Lang
  13. J. Mater. Sci. v.21 Preparation of Spherical fine ZnO particles by the spray pyrolysis using ultrasonic atomization technique T.Q. Liu;S. Sakurai;N. Mizutani;M. Kato