Microstructural Change in Rheocast AZ91D Magnesium Alloys with Stirring Rate and Isothermal Stirring Temperature

교반속도 및 등온교반온도에 따른 AZ91D 마그네슘합금 반응고 주조재의 미세조직 변화

  • 임창동 (한국기계연구원 재료기술연구부) ;
  • 신광선 (항공재료연구센터)
  • Published : 2003.06.20

Abstract

Rheocasting of AZ91D magnesium alloys yielded the microstructure consisted of the spherical primary particles in the matrix which is different from conventional casting. Rheocast ingots were produced under various processing conditions using batch type rheocaster. Morphology of primary particles was changed from rosette-shape to spherical shape with increasing stirring rate$(V_s)$ and decreasing isothermal stirring temperature$(T_s)$. With increasing $V_s$, more effective shearing between the particles occurred rather than the agglomeration and clustering, so the primary particle size decreased. But with decreasing $T_s$, primary particle size increased mainly due to sintering and partially Ostwald ripening. The sphericity of primary particles increased with increasing $V_s$ and decreasing $T_s$ due to enhanced abrasion among the primary particles. The uniformity of primary particle size increased with increasing Vs and $T_s$.

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References

  1. M. C. Flemings, R. G. Riek and K. P. Young : Mater Sci. & Eng., 'Rheocasting', 25 (1976) 103-117
  2. M. C. Flemings: Metall. Trans. A, 'Behavior of metal alloys in semisolid state', 22A (1991) 957-981
  3. D. H. Kim, Y. S. Han and H. I. Lee : J. Kor. Foundrymen's Soc., 'Development of semi-solid state process (I)-basic principles and characteristics', 12 (1992) 108-116
  4. D. H. Kirkwood : Int. Mat. Rev., 'Semisolid metal process-ing', 39 (1994) 173-189
  5. R. D. Doherty, H. I. Lee and E. A. Feest: Mater. Sci. & Eng., 'Microstructure of stir-cast metals', 65 (1984) 181-189
  6. Y. H. Yoo and D. H. Kim : J. Kor. Inst. Met. & Mater., 'Microstructure changes during isothermal shearing of semi-solid state Mg-Al-Zn alloys', 33 (1995) 437-446
  7. G. Wan and P. R. Sahm : Acta Metall. Mater., 'Ostwald ripening in the isothermal rheocasting process', 38 (1990) 967-972
  8. P. R. Prasad, S. Ray, J. L. Gaindhar and M. L. Kapoor : Z. Metallkde, 'Microstructure of rheocast hypoeutectic Al-Cu alloys', 73 (1982) 714-716
  9. C. D. yim, C. S. Kang and K. S. Shin : Proc. of the 2nd Pacific Rim Inter. Conf. on Advanced Materials and Pro-cessing, K. S. Shin, J. K. Yoon and S. J. Kim (Ed.), The Korean Institute of Metals and Materials (1995) 2269-2273
  10. A. Assar, N. El-Mallawy and M. A. Taha: Metals Technol-ogy, 'Influence of processing variables on structure and porosity in stir-casting Al-Cu alloys', 9 (1982) 165-170
  11. A. Tissier, D. Apelian and G. Regazzoni : J. Mater. Sci., 'Magnesium rheocasting : a study of processing-micro-structure interactions,' 25 (1990) 1184-1196
  12. P. R. Prasad, S. Ray, J. L. Gaindhar and M.L. Kapoor : Z. Metallkde, 'Effect of processing condition on the micro-structure of rheocast Al-Cu alloys', 80 (1989) 425-427
  13. P. R. Prasad, S. Ray, J. L. Gaindhar and M.L. Kapoor : J. Mater. Sci., 'Relation between processing, microstructure and mechanical properties of rheocast Al-Cu alloys', 23 (1988) 823-829
  14. G. Wan and P. R. Sahm : Acta. Metall. Mater., 'Particle growth by coalescence and Ostwald ripening in rheocasting of Pb-Sn', 38 (1990) 2367-2372
  15. W. Nan, S. Guangji and Y. Hanguo : J. Mater. Sci., 'Forma-tion and growth of solid particles in shear flow', 25 (1990)2185-2187