DOI QR코드

DOI QR Code

Mechanical Properties of (Y, Nb)-TZP/Alumina Composites for Dental Implant Abutments

치과 임플란트 상부구조물용 (Y, Nb)-TZP/알루미나 복합체의 기계적 물성

  • Published : 2004.07.01

Abstract

For abutment of dental implants, (Y, Nb)-TZP/Alumina composites were prepared by addition of 10-90 vol% alumina at an interval of 10 vol% into tetragonal zirconia solid solution which consists of 90.24 mol% Zr $O_2$, 5.31 mol% Y$_2$ $O_3$, and 4.45 mol% Nb$_2$O$\_$5/. Biaxial flexure strength and fracture toughness of composite were optimized by adding 10 vol% alumina, which resulted in 900 MPa and 8.9 MPam$\^$1/2/, respectively. The composite did not undergo low temperature degradation even after autoclave treatment at 200$^{\circ}C$ for 10 h. 65 of (Y, Nb)-TZP/Alumina composite abutments were employed into 40 patients and any adverse reaction, screw loosing, or fracture of abutments was not observed for the span of 2 years, indicating that the ceramic abutments can be safely used for restorations.

치과 임프란트의 상부구조물로 응용하기 위해 Zr $O_2$, $Y_2$ $O_3$, Nb$_2$ $O_{5}$를 각각 90.24, 5.31, 4.45mo1%씩 혼합한 정방정 지르코니아 고용체에 알루미나를 부피비로 10-90%를 10vo1%간격으로 첨가하여 (Y, Nb)-TZP/알루미나 복합체를 제조하였다. 최적의 기계적 물성은 알루미나를 10vo1% 첨가했을 때 이축 곡강도는 900MPa이었으며 파괴인성은 8.9MPam$^{1}$2/이었고 20$0^{\circ}C$ 오토크레이브하에서 10시간 열처리했을 때 저온열화가 관찰되지 않았다. 복합체를 임프란트 상부구조물로 제작하여 40명의 환자에게 총 65개를 시술한 후 2년 동안 관찰한 결과 부작용이나 나사의 풀림 또는 파절이 전혀 일어나지 않아 우수한 임상결과를 보였다.

Keywords

References

  1. J. Esthet. Dent. v.1 Esthetic High-Strength Implant Abutments: Part I and Part II V. Prestipino;A. Ingber
  2. Proct. Peridontic Esthet Dent. v.8 Implant-Supported Tooth Replacement in te Esthetic Region: A Complex Challenge U. Grunder;H. P. Spielman;T. Gaberthuel
  3. J. Esthet. Dent. v.6 All-Ceramic Implant Abutments : Esthetic Indications V. Prestipino;A. Ingber
  4. FDA
  5. FDA
  6. Biomaterials v.20 Mixed-Oxides Prosthetic Ceramic Ball Heads. Part 2 : Effect of the $ZrO_2$ Fraction on the Wear of Ceramic on Ceramic Joints S. Affatato;M. Testoni;G. L. Cacciari;A. Toni https://doi.org/10.1016/S0142-9612(99)00093-9
  7. Biomaterials v.22 Mixed-Oxides Prosthetic Ceramic Ball Heads. Part 3 : Effect of the $ZrO_2$ Fraction on the Wear of Ceramic on Ceramic Joint Prostheses. A Long-Term in Vitro Wear Study S. Affatato;M. Goldoni;M. Testoni;A. Toni https://doi.org/10.1016/S0142-9612(00)00235-0
  8. J. Biomed. Mater. Res. (Appl. Biomater) v.53 Mechanical Properties, Phase Stability, and Biocompatibility of (Y,Nb)-TZP/$Al_2O_3$ Composite Abutments for Dental Implant D. J. Kim;M. H. Lee;D. Lee;J. S. Han https://doi.org/10.1002/1097-4636(2000)53:4<438::AID-JBM19>3.0.CO;2-3
  9. Key Eng. Mater. v.240-242 Low Temperature Stability of Zirconia/Alumina Hip Joint Heads D. J. Kim;D. Lee;J. S. Han https://doi.org/10.4028/www.scientific.net/KEM.240-242.831
  10. Key Eng. Mater. v.254-256 Zirconia/Alumina Composite Dental Implant Abutments D. J. Kim;J. S. Han;S. H. Lee;J. H. Yang;D. Lee https://doi.org/10.4028/www.scientific.net/KEM.254-256.699
  11. ISO 6872, Dental Ceramic ISO
  12. J. Am. Ceram. Soc. v.64 A Critical Evaluation of Indentation Techniques for Measuring Fracture Toughness:I, Direct Crack Measurements G. R. Anstis;P. Chantikul;B. R. Lawn;d. B. Marshall https://doi.org/10.1111/j.1151-2916.1981.tb10320.x
  13. Quantitative Stereology E. E. Underwood
  14. J. Am. Ceram. Soc. v.81 no.9 Fracture Toughness Ionic Conductivity and Low Temperature Phase Stability of Tetragonal Zirconia Co-Doped with Yttria and Niobium Oxide D.-J. Kim;H.-J. Han;J.- W. Jang;H.-L. Lee https://doi.org/10.1111/j.1151-2916.1998.tb02626.x
  15. J. Am. Ceram. Soc. v.76 no.8 Raman Spectroscopy of Tetragonal Zirconia Solid solutions D.-J. Kim;H.-J. Jung; I.-S. Yang https://doi.org/10.1111/j.1151-2916.1993.tb08341.x
  16. J. Eur. Ceram. Soc. v.22 Influence of Alumina Particle Size on Fracture Toughness of (Y,Nb)-TZP/$Al_2O_3$ Composites D. Y. Lee;D.-J.Kim;B.-Y. Kim https://doi.org/10.1016/S0955-2219(02)00012-2
  17. Acta Metall v.34 Toughening of Brittle Solids by Martensitic Transformation A. G. Evans;R. M. Cannon https://doi.org/10.1016/0001-6160(86)90052-0
  18. J. Am. Ceram. Soc. v.78 Fracture Toughness of $Al_2O_3$-Particle-Dispersed $Y_2O_3$-Partially Stabilized Zirconia J.-F. Li;R. Watanabe https://doi.org/10.1111/j.1151-2916.1995.tb08441.x
  19. Adv. Mater. v.15 no.6 Percolative Mechanism of Aging in Zirconia-Containing Ceramics for Medical Applications C. Pecharrom;J. F. Bartolome;J. Requena;J. S. Moya;S. Deville;J. Chevalier;G. Frantozzi;R. Torrecillas https://doi.org/10.1002/adma.200390117
  20. Int. J. Prosthodont. v.14 no.5 Alumina Ceramic Implant Abutments Used for Single-Tooth Replacement : A Prospective 1-to 3-Year Multicenter Study B. Andersson;A. Tayler;B. Lang;H. Scheller;P. Sharer;J. Sorensen;D. Tarnow
  21. Int. J. Prosthodont. v.12 Ceramic Implant Abutments Used for Short-Span Fixed Partial Dentures : A Prospective 2-Year Multicenter Study B. Andersson;P. Sharer;M. Simion;C. Bergstrom

Cited by

  1. Cracking of densely coated layer adhesively bonded to porous substrates under Hertzian stress vol.42, pp.21, 2007, https://doi.org/10.1007/s10853-007-2063-2