Concentration of Heavy Metals, Residual Pesticides and Sulfur Dioxide before/after a Decoction - In Prescription consist of Sipjeondaebo-tang -

전탕 전과 후의 중금속, 잔류농약 및 잔류이산화황의 농도변화 - 십전대보탕 구성처방을 중심으로 -

  • Seo, Chang-Seob (Division of Standard Research, Korea Institute of Oriental Medicine) ;
  • Huang, Dae-Sun (Division of Standard Research, Korea Institute of Oriental Medicine) ;
  • Lee, Jun-Kyoung (Division of Standard Research, Korea Institute of Oriental Medicine) ;
  • Ha, Hye-Kyung (Division of Standard Research, Korea Institute of Oriental Medicine) ;
  • Chun, Jin-Mi (Division of Standard Research, Korea Institute of Oriental Medicine) ;
  • Um, Young-Ran (Division of TKM Integrated Research, Korea Institute of Oriental Medicine) ;
  • Jang, Seol (Herbal Quality Control Center, Korea Institute of Oriental Medicine) ;
  • Shin, Hyeun-Kyoo (Division of Standard Research, Korea Institute of Oriental Medicine)
  • 서창섭 (한국한의학연구원 표준화연구본부) ;
  • 황대선 (한국한의학연구원 표준화연구본부) ;
  • 이준경 (한국한의학연구원 표준화연구본부) ;
  • 하혜경 (한국한의학연구원 표준화연구본부) ;
  • 천진미 (한국한의학연구원 표준화연구본부) ;
  • 엄영란 (한국한의학연구원 한의융합연구본부) ;
  • 장설 (한국한의학연구원 한약품질관리센터) ;
  • 신현구 (한국한의학연구원 표준화연구본부)
  • Published : 2009.07.31

Abstract

Objective: To compare the contents of heavy metals, residual pesticides and sulfur dioxide before/after a decoction. Methods: The heavy metal contents before/after a decoction were measured by inductively-coupled plasma atomic emission spectrometer (ICP-AES) and mercury analyzer. In order to analyze pesticides in 5 samples we used simultaneous multi-residue analysis of pesticides by GC/ECD, which was followed by GC/MSD analysis to confirm the identity of the detected pesticide in each sample. In addition, the contents of sulfur dioxide ($SO_2$) were performed by Monier-Williams distillation method. Results: 1. The mean values of heavy metal contents (mg/kg) for the samples were as follows: Sipjeondaebo-tang (before decoction - Pb; 1.163, Cd; 0.257, As; 0.080 and Hg; 0.016, after decoction - Pb; 0.059, Cd; 0.007, As; 0.006 and Hg; 0.0003), Palmul-tang (before decoction - Pb; 1.181, Cd; 0.242, As; 0.152 and Hg; 0.014, after decoction - Pb; 0.067, Cd; 0.008, As; 0.008 and Hg; 0.0003), Sagunja-tang (before decoction - Pb; 1.285, Cd; 0.283, As; 0.063 and Hg; 0.012, after decoction - Pb; 0.047, Cd; 0.009, As; 0.004 and Hg; not detected) and Samul-tang (before decoction - Pb; 1.025, Cd; 0.169, As; 0.099 and Hg; 0.013, after decoction - Pb; 0.065, Cd; 0.007, As; 0.010 and Hg; 0.001). 2. Contents (mg/kg) of residual pesticides before/after a decoction were not detected in any samples. 3. Contents (mg/kg) of sulfur dioxide ($SO_2$) before a decoction in Sipjeondaebo-tang, Palmul-tang, Sagunja-tang and Samul-tang exhibited 5.0, 6.0, 14.0 and 6.9, respectively. However, contents of sulfur dioxide after a decoction were not detected in any samples. Conclusion: These results will be used to establish a criterion for heavy metals, residual pesticides and sulfur dioxide.

Keywords

References

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