Journal of the Korean Applied Science and Technology (한국응용과학기술학회지)

The Korean Society of Applied Science and Technology (한국응용과학기술학회)
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Synthesis and Characteristic of Ferric Ferrocyanide Coated Titania/Mica Pearlescent Pigments by Hydrothermal Synthesis Method

수열 합성법에 의해 페릭페로시아나이드가 코팅된 마이카 티나니아 진주광택안료의 합성 및 특성

  • Lee, Kwan-Sik (Department of Engineering Chemistry, Chungbuk National University) ;
  • Lee, Dong-Kyu (Department of Engineering Chemistry, Chungbuk National University)
  • 이관식 (충북대학교 공과대학 공업화학과) ;
  • 이동규 (충북대학교 공과대학 공업화학과)
  • Received : 2011.09.04
  • Accepted : 2011.09.29
  • Published : 2011.09.30
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Abstract

The pearlesent pigment has received attention in a diversity of fields like cosmetics, inks, paints and so on. Ferric Ferrocyanide, one of the nano sized pearlescent pigment, is a kind of surface modification pigment that covers a metal oxidized substance or a coloring agent with uniform thickness. Characteristics of pearlescent pigment are various interference color, intense gloss effect and a three-dimensional effect. We synthesised the pearlesent pigment that ferric ferrocyanide can be deposited on the titania/mica surface by hydrothermal synthesis method. The process parameters are concentration of precursor, controlling pH and reaction temperature. The optimun conditions is that amount of iron(III) chloride hexahydrate is 3.1 wt% and amount of potassim ferrocynide trihydrate is 3.6 wt% in the started pH 4.5 at $70^{\circ}C$. The coating rate and coating efficiency of ferric ferrocyanide was about 1.47 % and 96.7 %, respectively. The synthesised pearlesent pigment was characterized by SEM, XRD, FT-IR and EDS.

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References

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