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Effect of $Na_2SiO_3$ Concentration on the Properties of AZ31 Magnesium Alloy Prepared by Electrolytic Plasma Processing

  • Ahn, Byung-Hyun (School of Nano & Advance Material Engineering, Changwon National University) ;
  • Lee, Dong-Gun (School of Nano & Advance Material Engineering, Changwon National University) ;
  • Cho, Ho-Je (School of Nano & Advance Material Engineering, Changwon National University) ;
  • Lee, Seung-Rok (School of Nano & Advance Material Engineering, Changwon National University) ;
  • Ahmed, Faheem (School of Nano & Advance Material Engineering, Changwon National University) ;
  • Anwar, M.S. (School of Nano & Advance Material Engineering, Changwon National University) ;
  • Koo, Bon-Heun (School of Nano & Advance Material Engineering, Changwon National University)
  • Published : 2013.11.20

Abstract

The effect of $Na_2SiO_3$ concentration on the dense ceramic oxide coatings prepared on a AZ31 magnesium alloy through electrolytic plasma processing in a NaOH-$Na_2SiF_6$ electrolytic solution, have been investigated. The x-ray diffraction (XRD) results showed that the coating formed in silicate electrolyte was mainly composed of MgO, $Na_2SiO_4$. Scanning electron microscopy (SEM) micrographs reveals that the number of pores on coatings decreases by increasing concentration of $Na_2SiO_3$ and coatings prepared in 12 - 20 g/L of $Na_2SiO_3$ show similar surface morphologies. The observed micro-hardness of coating layers is over 1000 Hv, which is much larger than that of the original AZ31 magnesium alloy without electrolytic plasma processing.

Keywords

References

  1. T. Nakada, Electron. Mater. Lett. 8, 179 (2012). https://doi.org/10.1007/s13391-012-2034-x
  2. M. S. Anwar, S. Kumar, F. Ahmed, G. W. Kim, and B. H. Koo, J. Nanosci. Nanotech. 12, 5523 (2012). https://doi.org/10.1166/jnn.2012.6327
  3. Z.Q. Qi, J. C. Jiang, and E. I. Meletis, J. Nanosci. Nanotech. 9, 4227 (2009). https://doi.org/10.1166/jnn.2009.M37
  4. B. L. Mordike and T. Ebert, Mater. Sci. Eng. A, 302, 37 (2001). https://doi.org/10.1016/S0921-5093(00)01351-4
  5. E. Aghion, B. Bronfin, and D. Eliezer, J. Mater. Process. Technol. 117, 381 (2001). https://doi.org/10.1016/S0924-0136(01)00779-8
  6. H. F. Guo, M. Z. An, S. Xu, and H. B. Huo, Thin Solid Films 485, 53 (2005). https://doi.org/10.1016/j.tsf.2005.03.050
  7. H. P. Duan, C. W. Yan, and F. H. Wang, Electrochim. Acta 52, 5002 (2007). https://doi.org/10.1016/j.electacta.2007.02.021
  8. A. L Yerokhin, T. A. Shatrov, V. Samsonov, P. Shashkov, A. Pilkingtor A. Leyland, and A. Matthews, Surf. Coat. Technol. 199, 150 (2005). https://doi.org/10.1016/j.surfcoat.2004.10.147
  9. I. V. Lukiyanchuk, V. G. Kuryavyi, D. L. Boguta, S. B. Bulanova, and P. S. Gordienko, Thin Solid Films 446, 54 (2004). https://doi.org/10.1016/S0040-6090(03)01318-X
  10. W. Xue, C. Wang, H. Tian, and Y. Lai, Surf. Coat. Technol. 201, 8695 (2007). https://doi.org/10.1016/j.surfcoat.2006.10.029
  11. Y. M Wang, D. C. Jia, L. X. Guo, T. Q. Lei, and B. L. Jiang, Mater. Chem. Phys. 90, 128 (2005). https://doi.org/10.1016/j.matchemphys.2004.10.025
  12. J. Liang, B. Guo, J. Tian, H. Liu, J. Zhou, and T. Xu, Appl. Surf. Sci. 252, 345 (2005). https://doi.org/10.1016/j.apsusc.2005.01.007
  13. A. Ghasemi, V. S Raja, C. Blawert, W. Dietzel, and K. U. Kainer, Surf. Coat. Technol. 202, 3513 (2008). https://doi.org/10.1016/j.surfcoat.2007.12.033
  14. J. Liang, B. G. Guo, J. Tian, H. W. Liu, J. F. Zhou, and T. Xu, Appl. Surf. Sci. 252, 345 (2005). https://doi.org/10.1016/j.apsusc.2005.01.007
  15. H. F. Guo and M. Z. An, Appl. Surf. Sci. 246, 229 (2005). https://doi.org/10.1016/j.apsusc.2004.11.031
  16. H. Chen, G. H. Lv, G. L. Zhang, H. Pang, X. Q. Wang, and S. Z. Yang, Surf. Coat. Technol. 205, S32 (2010). https://doi.org/10.1016/j.surfcoat.2010.03.032

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