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Freeze-thawing Conditions to Produce High Quality Bokbunja (Rubus occidentalis)

냉동유통 고품질 복분자 생산을 위한 냉해동 조건 연구

  • Kim, Jung-Eun (Department of Food Science and Technology, Chungnam National University) ;
  • Jo, Hye-Jin (Department of Food Science and Technology, Chungnam National University) ;
  • Yu, Min-Ji (Department of Food Science and Technology, Chungnam National University) ;
  • Song, Kyung Bin (Department of Food Science and Technology, Chungnam National University) ;
  • Kim, Ha-Yun (Department of Agrofood Resources, National Academy of Agricultural Science, Rural Development Administration) ;
  • Hwang, In Guk (Department of Agrofood Resources, National Academy of Agricultural Science, Rural Development Administration) ;
  • Yoo, Seon Mi (Department of Agrofood Resources, National Academy of Agricultural Science, Rural Development Administration) ;
  • Han, Gwi Jung (Department of Agrofood Resources, National Academy of Agricultural Science, Rural Development Administration) ;
  • Park, Jong-Tae (Department of Food Science and Technology, Chungnam National University)
  • 김정은 (충남대학교 식품공학과) ;
  • 조혜진 (충남대학교 식품공학과) ;
  • 유민지 (충남대학교 식품공학과) ;
  • 송경빈 (충남대학교 식품공학과) ;
  • 김하윤 (농촌진흥청 국립농업과학원 농식품자원부) ;
  • 황인국 (농촌진흥청 국립농업과학원 농식품자원부) ;
  • 유선미 (농촌진흥청 국립농업과학원 농식품자원부) ;
  • 한귀정 (농촌진흥청 국립농업과학원 농식품자원부) ;
  • 박종태 (충남대학교 식품공학과)
  • Received : 2014.10.23
  • Accepted : 2014.11.05
  • Published : 2014.12.31

Abstract

To date, the quality and safety of frozen bokbunja have not been clearly assessed. To produce high-quality frozen bokbunja, the optimal freeze-thaw conditions need to be explored. The most popular cultivar (Rubus occidentalis) in Korea was selected for this study. To determine the changes in the quality of frozen R. occidentalis berries, different freezing temperatures were used. The berries were frozen at -20, -45, and $-70^{\circ}C$ immediately after harvest. The drip ratio, hardness, pH, sugar content, color, and anthocyanidin content of the frozen and thawed samples were analyzed. The drip ratio, sugar content, and hardness of the berries correlated significantly with the freezing temperatures. The color and pH of the berries were not significantly affected by the freezing conditions. Frozen leaks between cells reduced significantly with decreasing temperatures. The freeze-thawing process significantly reduced the total aerobic bacteria and inhibited the growth of yeast/mold in the berries to about 2 log scales.

냉동 복분자의 품질에 대한 연구가 매우 부족하고 고품질 냉동 복분자를 생산하기 위한 냉해동 최적조건 연구가 시급히 필요한 실정이다. 본 연구에서는 국내에서 가장 많이 재배되는 R. occidentalis의 성숙과를 이용하여 냉해동 연구를 수행하였다. 복분자를 수확 직 후 -20, -45, $-70^{\circ}C$ 조건에서 냉동하고 2개월 동안 $-20^{\circ}C$에서 저장한 후 $4^{\circ}C$ 혹은 상온에서 해동하여 복분자의 품질변화를 drip률, 강도, pH, 유리당 함량, 색도 및 anthocyanidin 함량을 중심으로 분석하였다. 분석결과, 냉동 온도에 따라 drip률, 유리당 함량 및 과의 강도가 유의적인 차이가 나타나는 것으로 측정되었다. 그러나 색도, pH, anthocyanidin의 함량 등은 냉동 조건에 따른 변화가 뚜렷하게 나타나지 않았다. 냉동 단면을 비교한 결과, 낮은 온도에서 냉동할수록 세포간 유출수가 현저하게 감소하는 것으로 관찰되었다. 미생물의 오염도는 호기성세균은 물론 효모와 곰팡이도 냉해동을 거치면서 유의적으로 감소하는 것을 확인 할 수 있었다.

Keywords

References

  1. Kwon KH, Cha WS, Kim DC, Shin HJ. A research and application of active ingredients in bokbunja (Rubus coreanus Miquel). Korean J. Biotechnol. Bioeng. 21: 405-409 (2006)
  2. Kim JM, Shin MS. Characteristics of Rubus coreanus Miq. fruits at different ripening stages. Korean J. Food Sci. Technol. 43: 341-347 (2011) https://doi.org/10.9721/KJFST.2011.43.3.341
  3. Kim YJ, Han SH, Jeon JY, Hwang MH, Im YJ, Chae SW, Kim MG. Method development of ellagic acid as marker compound for standardization of Gochang bokbunja (Rubus coreanus Miquel) as functional ingredient. J. Korean Soc. Food Sci. Nutr. 41: 1554-1558 (2012) https://doi.org/10.3746/jkfn.2012.41.11.1554
  4. Sung KC. A study on the pharmaceutical & chemical characteristics and analysis of natural bokbunja extract. J. Korean Oil Chemists' Soc. 29: 402-411 (2012)
  5. Lee JH, Choi HR, Lee SJ, Lee MJ, Ko YJ, Kwon JW, Lee HK, Jeong JT, Lee TB. Blood pressure modulating effects of black raspberry extracts in vitro and in vivo. Korean J. Food Sci. Technol. 46: 375-383 (2014) https://doi.org/10.9721/KJFST.2014.46.3.375
  6. Choi HR, Lee JH, Lee SJ, Lee MJ, Jeong JT, Lee TB. Effects of unripe black raspberry water extract on lipid metabolism and oxidative stress in mice. Korean J. Food Sci. Technol. 46: 489-497 (2014) https://doi.org/10.9721/KJFST.2014.46.4.489
  7. Lee SJ. Physico-chemical characteristics of black raspberry fruits (bokbunja) and wines in Korea. Korean J. Food Sci. Technol. 45: 451-459 (2013) https://doi.org/10.9721/KJFST.2013.45.4.451
  8. Lee SJ. Volatile analysis of commercial Korean black raspberry wines (bokbunjaju) using headspace solid-phase microextraction. Korean J. Food Sci. Technol. 46: 425-431 (2014) https://doi.org/10.9721/KJFST.2014.46.4.425
  9. Lee JS, Choi HY, Bae IH. Quality properties of yoghurt added with bokbunja (Rubus coreanus Miquel) wine. Korean J. Food Sci. An. 33: 806-816 (2013) https://doi.org/10.5851/kosfa.2013.33.6.806
  10. Jin TY, Quan WR, Wang MH. Manufacturing characteristics and physicochemical component analysis of bokbunja (Rubus coreanus Miquel) jelly. J. Korean Soc. Food Sci. Nutr. 39: 554-559 (2010) https://doi.org/10.3746/jkfn.2010.39.4.554
  11. Jin TY, Heo SI, Lee WG, Lee IS, Wang MH. Manufacturing characteristics and physicochemical component analysis of bokbunja (Rubus coreanus Miquel) jam. J. Korean Soc. Food Sci. Nutr. 37: 48-52 (2008) https://doi.org/10.3746/jkfn.2008.37.1.48
  12. Seo SH, Yoo SA, Kang BS, Son HS. Quality characteristics of Korean black raspberry bokbunja wines produced using different amounts of water in the fermentation process. Korean J. Food Sci. Technol. 46: 33-38 (2014) https://doi.org/10.9721/KJFST.2014.46.1.33
  13. Yu OK, Kim JE, Cha YS. The quality characteristics of jelly added with bokbunja (Rubus coreanus Miquel). J. Korean Soc. Food Sci. Nutr. 37: 792-797 (2008) https://doi.org/10.3746/jkfn.2008.37.6.792
  14. Bobinaite R, Viskelis P, Venskutonis PR. Variation of total phenolics, anthocyanins, ellagic acid and radical scavenging capacity in various raspberry (Rubus spp.) cultivars. Food Chem. 132: 1495-1501 (2012) https://doi.org/10.1016/j.foodchem.2011.11.137
  15. Chen L, Xin X, Zhang H, Yuan Q. Phytochemical properties and antioxidant capacities of commercial raspberry varieties. J. Funct. Foods 5: 508-515 (2013) https://doi.org/10.1016/j.jff.2012.10.009
  16. Gu J, Ahn-Jarvis JH, Riedl KM, Schwartz SJ, Clinton SK, Vodovotz Y. Characterization of black raspberry functional food products for cancer prevention human clinical trials. J. Agr. Food Chem. 62: 3997-4006 (2013)
  17. Ku CS, Mun SP. Antioxidant activities of ethanol extracts from seeds in fresh bokbunja (Rubus coreanus Miq.) and wine processing waste. Bioresource Technol. 99: 4503-4509 (2008) https://doi.org/10.1016/j.biortech.2007.08.063
  18. Moon Y-S, Han J-H, Lee T-B, Kwon J-W, Choi C-H. Lipid-modulating effects of aqueous extract of Rubus occidentalis in hepatocarcinoma HepG2 cells. Am. J. Biosci. 2: 64-69 (2014)
  19. Choung MG, Lim JD. Antioxidant, anticancer and immune activation of anthocyanin fraction from Rubus coreanus Miquel fruits (bokbunja). Korean J. Medicinal Crop Sci. 20: 259-269 (2012) https://doi.org/10.7783/KJMCS.2012.20.4.259
  20. Cha HS, Youn AR, Park PJ, Choi HR, Kim BS. Physicochemical characteristics of Rubus coreanus Miquel during maturation. Korean J. Food Sci. Technol. 39: 476-479 (2007)
  21. Youn AR, Kwon KH, Kim BS, Noh BS, Cha HS. Quality changes in Rubus coreanus Miquel during frozen storage. Korean J. Food Preserv. 16: 618-622 (2009)
  22. Kim JW, Lee GH, Hur JH. Quality characteristics of citron jam made with frozen citron in Korea. Korean J. Food Sci. Technol. 38: 197-201 (2006)
  23. Yoon AR, Kwon KH, Kim BS, Kim SH, Noh BS, Cha HS. Changes in quality of muskmelon (Cucumis melo L.) during storage at different temperatures. Korean J. Food Sci. Technol. 41: 251-257 (2009)
  24. de Ancos B, Ibanez E, Reglero G, Cano MP. Frozen storage effects on anthocyanins and volatile compounds of raspberry fruit. J. Agr. Food Chem. 48: 873-879 (2000) https://doi.org/10.1021/jf990747c
  25. Hunter KJ, Fletcher JM. The antioxidant activity and composition of fresh, frozen, jarred and canned vegetables. Innov. Food Sci. Emerg. 3: 399-406 (2002) https://doi.org/10.1016/S1466-8564(02)00048-6
  26. Kidmose U, Martens HJ. Changes in texture, microstructure and nutritional quality of carrot slices during blanching and freezing. J. Sci. Food Agr. 79: 1747-1753 (1999) https://doi.org/10.1002/(SICI)1097-0010(199909)79:12<1747::AID-JSFA429>3.0.CO;2-B
  27. Chassagne-Berces S, Poirier C, Devaux M-F, Fonseca F, Lahaye M, Pigorini G, Girault C, Marin M, Guillon F. Changes in texture, cellular structure and cell wall composition in apple tissue as a result of freezing. Food Res. Int. 42: 788-797 (2009) https://doi.org/10.1016/j.foodres.2009.03.001
  28. Otero L, Solas MT, Sanz PD, de Elvira C, Carrasco JA. Contrasting effects of high-pressure-assisted freezing and conventional airfreezing on eggplant tissue microstructure. Z. Lebensm. Unters. F. A. 206: 338-342 (1998) https://doi.org/10.1007/s002170050269
  29. Kim JY, Lee MY, Ji GE, Lee YS, Hwang KT. Production of aaminobutyric acid in black raspberry juice during fermentation by Lactobacillus brevis GABA100. Int. J. Food Microbiol. 130: 12-16 (2009) https://doi.org/10.1016/j.ijfoodmicro.2008.12.028
  30. Cha HS, Lee MK, Hwang JB, Park MS, Park KM. Physicochemical characteristics of Rubus coreanus Miquel. J. Korean Soc. Food Sci. Nutr. 30: 1021-1025 (2001)
  31. Paudel L, Wyzgoski FJ, Giusti MM, Johnson JL, Rinaldi PL, Scheerens JC, Chanon AM, Bomser JA, Miller AR, Hardy JK. NMR-based metabolomic investigation of bioactivity of chemical constituents in black raspberry (Rubus occidentalis L.) fruit extracts. J. Agr. Food Chem. 62: 1989-1998 (2014) https://doi.org/10.1021/jf404998k
  32. Lee J, Dossett M , Finn CE. Rubus fruit phenolic research: The good, the bad, and the confusing. Food Chem. 130: 785-796 (2012) https://doi.org/10.1016/j.foodchem.2011.08.022

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