Metals and materials international

The Korean Institute of Metals and Materials (대한금속재료학회)
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Interfacial Microstructure and Shear Strength of Reactive Air Brazed Oxygen Transport Membrane Ceramic-Metal Alloy Joints

  • Muhamad FR, Wahid (School of Materials Science and Engineering, Yeungnam University) ;
  • Yoon, Dang-Hyok (School of Materials Science and Engineering, Yeungnam University) ;
  • Raju, Kati (School of Materials Science and Engineering, Yeungnam University) ;
  • Kim, Seyoung (Energy Efficiency and Materials Research Division, Korea Institute of Energy Research) ;
  • Song, Kwang-sup (Energy Efficiency and Materials Research Division, Korea Institute of Energy Research) ;
  • Yu, Ji Haeng (Energy Efficiency and Materials Research Division, Korea Institute of Energy Research)
  • Received : 2017.03.04
  • Accepted : 2017.06.24
  • Published : 2018.01.31
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Abstract

To fabricate a multi-layered structure for maximizing oxygen production, oxygen transport membrane (OTM) ceramics need to be joined or sealed hermetically metal supports for interfacing with the peripheral components of the system. Therefore, in this study, Ag-10 wt% CuO was evaluated as an effective filler material for the reactive air brazing of dense $Ce_{0.9}Gd_{0.1}O_{2-{\delta}}-La_{0.7}Sr_{0.3}MnO_{3{\pm}{\delta}}$ (GDC-LSM) OTM ceramics. Thermal decomposition in air and wetting behavior of the braze filler was performed. Reactive air brazing was performed at $1050^{\circ}C$ for 30 min in air to join GDC-LSM with four different commercially available high temperature-resistant metal alloys, such as Crofer 22 APU, Inconel 600, Fecralloy, and AISI 310S. The microstructure and elemental distribution of the ceramic-ceramic and ceramic-metal interfaces were examined from polished cross-sections. The mechanical shear strength at room temperature for the as-brazed and isothermally aged ($800^{\circ}C$ for 24 h) joints of all the samples was compared. The results showed that the strength of the ceramic-ceramic joints was decreased marginally by aging; however, in the case of metal-ceramic joints, different decreases in strengths were observed according to the metal alloy used, which was explained based on the formation of different oxide layers at the interfaces.

Keywords

Acknowledgement

Supported by : Korea Institute of Energy Research (KIER)

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