Journal of Industrial and Engineering Chemistry

  • Volume 59
  • /
  • Pages.8-16
  • /
  • 2018
  • /
  • 1226-086X(pISSN)
  • /
  • 1876-794X(eISSN)
The Korean Society of Industrial and Engineering Chemistry (한국공업화학회)
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Controlled deposition of MOFs by dip-coating in thin film nanocomposite membranes for organic solvent nanofiltration

  • Sarango, Lilian (Chemical and Environmental Engineering Department and Instituto de Nanociencia de Aragon (INA), Universidad de Zaragoza) ;
  • Paseta, Lorena (Chemical and Environmental Engineering Department and Instituto de Nanociencia de Aragon (INA), Universidad de Zaragoza) ;
  • Navarro, Marta (Chemical and Environmental Engineering Department and Instituto de Nanociencia de Aragon (INA), Universidad de Zaragoza) ;
  • Zornoza, Beatriz (Chemical and Environmental Engineering Department and Instituto de Nanociencia de Aragon (INA), Universidad de Zaragoza) ;
  • Coronas, Joaquin (Chemical and Environmental Engineering Department and Instituto de Nanociencia de Aragon (INA), Universidad de Zaragoza)
  • Received : 2017.06.14
  • Accepted : 2017.09.28
  • Published : 2018.03.31
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Abstract

ZIF-8 and ZIF-67 particles, with sizes of $70{\pm}10nm$ and $240{\pm}40nm$, respectively, were deposited by dip-coating on top of polyimide $P84^{(R)}$ asymmetric supports. In the best conditions, this gives rise to a MOF (metal-organic framework) monolayer which remains on the polyimide support during the interfacial polymerization of polyamide carried out to produce a thin film nanocomposite membrane for organic solvent nanofiltration (OSN). This method is simple, shorter and is environmentally friendly, since no excess MOF is lost during the interfacial polymerization, exhibiting good OSN results: dye rejection of 90% together with a high methanol permeance of $8.7Lm^{-2}h^{-1}bar^{-1}$.

Keywords

Acknowledgement

Supported by : Spanish Ministry of Economy and Competitiveness (MINECO), FEDER

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