Electronic Materials Letters

The Korean Institute of Metals and Materials (대한금속재료학회)
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Effect of Milling on Properties and Consolidation of AlN by High-Frequency Induction Heated Sintering

  • Shon, In-Jin (Division of Advanced Materials Engineering and Center for Advanced Bioimaging Research, Engineering College, Chonbuk National University) ;
  • Kwon, Hanjung (Minerals and Materials Processing Division, Korea Institute of Geoscience, Mining and Materials Resources) ;
  • Oh, Hyun-Su (Division of Advanced Materials Engineering and Center for Advanced Bioimaging Research, Engineering College, Chonbuk National University)
  • Received : 2013.06.20
  • Accepted : 2013.07.23
  • Published : 2014.03.20
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Abstract

Commercial AlN powders were high-energy ball milled for various durations, and consolidated without a binder, using the high-frequency induction heated sintering method (HFIHS). The effect of milling on the sintering behavior, crystallite size and mechanical properties of AlN compacts were evaluated. A dense AlN compact with a relative density of up to 96% could be readily obtained within 1 min. The ball milling effectively refined the crystallite structure of AlN powders, and facilitated the subsequent densification. The sinter-onset temperature was reduced appreciably, by the prior milling for 10 h from $750^{\circ}C$ to $600^{\circ}C$. Accordingly, the relative density of AlN compact increased, as the milling time increased. It is clearly demonstrated that a quick densification of AlN bulk materials to near the theoretical density could be obtained by the combination of HFIHS and the preparatory high-energy ball milling process.

Keywords

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