Electronic Materials Letters

The Korean Institute of Metals and Materials (대한금속재료학회)
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Effect of Milling on Properties and Consolidation of $TiO_2$ by High-Frequency Induction Heated Sintering

  • Shon, In-Jin (Division of Advanced Materials Engineering and the Research Center of Advanced Materials Development, Engineering College, Chonbuk National University) ;
  • Lee, Geon-Woo (Division of Advanced Materials Engineering and the Research Center of Advanced Materials Development, Engineering College, Chonbuk National University) ;
  • Doh, Jung-Mann (Interface Control Research Center, Korea Institute of Science and Technology) ;
  • Yoon, Jin-Kook (Interface Control Research Center, Korea Institute of Science and Technology)
  • Published : 2013.03.20
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Abstract

Commercial $TiO_2$ powders were high-energy ball milled for various durations and consolidated using high-frequency induction heated sintering (HFIHS). The effect of milling on the sintering behavior, crystallite size and mechanical properties of $TiO_2$ powders were evaluated. A nanostructured dense $TiO_2$ compact with a relative density of up to 98% was readily obtained within 1 min. The ball milling effectively refined the crystallite structure of $TiO_2$ powders and facilitated the subsequent densification. The sinter-onset temperature was noticeably reduced by the prior milling for 10 h. Accordingly, the relative density of $TiO_2$ compact increased as the milling time increases. Furthermore, the microhardness and fracture toughness of sintered $TiO_2$ increased as the density increases. It is clearly demonstrated that a quick densification of nano-structured $TiO_2$ bulk materials to near theoretical density could be obtained by the combination of HFIHS and the preparatory high-energy ball milling processes.

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